Please wait a minute...
J4  2011, Vol. 45 Issue (5): 928-933    DOI: 10.3785/j.issn.1008-973X.2011.05.026
化学工程、材料工程     
快速热处理对高能粒子辐照硅中氧沉淀的影响
陈贵锋,马晓薇,吴建海,马巧云,薛晶晶,郝秋艳
河北工业大学 材料学院, 河北省新型功能材料实验室,天津 300130
Effect of rapid thermal process on oxygen precipitates behavior in
silicon irradiated by high energy particles
CHEN Gui-feng, MA Xiao-wei, WU Jian-hai, MA Qiao-yun,
XUE Jing-jing, HAO Qiu-yan
Key Lab. for new type of functional materials in Hebei Province, School of Material Science and Engineering,
Hebei University of Technology, Tianjin 300130, China
 全文: PDF  HTML
摘要:

研究快速热处理对快中子辐照掺氮直拉硅(NCZ-Si )和电子辐照直拉硅(CZ-Si)中氧沉淀和清洁区(DZ )的影响.样品经过不同温度、降温速率和退火气氛快速热处理(RTP)预处理后,再进行高温一步长时间退火,以形成氧沉淀.研究结果表明:对于快中子辐照NCZ-Si,RTP有助于后期退火中DZ的生成,且RTP温度越高,形成的DZ越宽;而高的降温速率会使得DZ宽度变窄;对于电子辐照CZ-Si,在N2气氛下高温RTP更能促进氧沉淀形成,体缺陷(bulk micro defects,BMDS)密度较大.

Abstract:

The oxygen precipitation behavior has been investigated in nitrogen-doped Czochralski silicon (NCZ-Si) irradiated by fastneutron and Czochralski silicon (CZ-Si) irradiated by electron after Rapid Thermal Process (RTP). The samples irradiated by fast-neutron or electron with different dose were treated by post-annealing after RTP pre-annealing at different temperature, cooling rate and ambient. It is found that the RTP process conduces to the denuded zone (DZ) form during the post-annealing treatment in fast-neutron irradiated NCZ-Si wafer. Furthermore, the DZ is getting wider with increasing RTP temperature. On the contrary, the DZ narrowed at high cooling rate. For another thing, the RTP process under N2 ambient in electron irradiated CZ-Si wafer is easy to form the oxygen precipitates and lead to higher density bulk microdefects (BMDS).

出版日期: 2011-11-24
:  TU 411  
基金资助:

国家自然科学基金资助项目(50872028);河北省自然科学基金资助项目(E2008000079);河北省教育厅科研计划资助项目(2009318).

作者简介: 陈贵锋(1979-),河北唐山人,讲师,从事半导体缺陷工程研究.E-mail: admat@hebut.edu.cn
服务  
把本文推荐给朋友
加入引用管理器
E-mail Alert
作者相关文章  

引用本文:

陈贵锋,马晓薇,吴建海,马巧云,薛晶晶,郝秋艳. 快速热处理对高能粒子辐照硅中氧沉淀的影响[J]. J4, 2011, 45(5): 928-933.

CHEN Gui-feng, MA Xiao-wei, WU Jian-hai, MA Qiao-yun, XUE Jing-jing, HAO Qiu-yan. Effect of rapid thermal process on oxygen precipitates behavior in
silicon irradiated by high energy particles. J4, 2011, 45(5): 928-933.

链接本文:

https://www.zjujournals.com/eng/CN/10.3785/j.issn.1008-973X.2011.05.026        https://www.zjujournals.com/eng/CN/Y2011/V45/I5/928

[1] 李养贤,刘何燕,牛萍娟,等. 中子辐照直拉硅中的本征吸除效应[J]. 物理学报, 2002, 51(10): 24072410.
LI Yangxian, LIU Heyan, NIU Pingjuan, et al. The intrinsic gettering in neutron irradiation Czochralskisilicon [J]. Acta Physica Sinica, 2002, 51(10):2410.
[2] SUEZAWA M, SUMINO K, HARADA H, et al. Nitrogenoxygen complexes as shallow donors in silicon crystals [J]. Jpan. Journal of Applied Physics, 1986, 25(52/54): L859-L864.
[3] JIANG Hanqin, MA Xiangyang, YANG Deren, et al. Effect of vacancy on nucleation for oxygen precipitation in conventional and nitrogendoped Czochralski silicon [J]. Journal of Semiconductors, 2008, 29(10): 1984-1987.
[4] LI Yangxian, JU Yulin, LIU Caichi, et al. Inhibition of neutron irradiation on oxidation stacking faults on the surface of Si wafers [J]. J.Cryst.Growth, 1996, 160(3/4): 250-252.
[5] LI Yangxian, GUO H Y, LIU Heyan, et al. The effects of neutron irradiation on the oxygen precipitation in Czochralskisilicon [J]. J.Cryst.Growth, 2003, 253(1/4): 6-9.
[6] Chen Guifeng, LI Yangxian, LI Xinghua, et al. Influence of rapid thermal process on intrinsic gettering in fast neutron irradiated Czochralski silicon [J]. Transactions of Nonferrous Metals Society of China, 2006, 16(1): 109-112.
[7] CHEN Guifeng, MA Xiaowei, BAI Yunna, et al. Effect of oxygen precipitates in annealed electron irradiated Czochralski silicon [C]∥ ISTC/CSTIC 2009 International Semiconductor Technology Conference. Shanghai: The Electrochemical Society, 2009,52-54.
[8] 马巧云. 快中子辐照直拉硅中氧沉淀及诱生缺陷研究[D]. 天津:河北工业大学, 2005: 12-15.
MA Qiaoyun. Investigation of oxygen precipitation and induceddefects in fast neutron irradiated Czochralski silicon [D]. Tianjin: Hebei University of Technology, 2005: 12-15.
[9] QI M W, TAN S S, ZHU B, et al. The evidence for interaction of the NN pair with oxygen in Czochralski silicon [J]. Journal of Applied Physics, 1991, 69: 3775-3777.

[10] SURMA B, LONDOS C A, EMTSEV V V, et al. Infrared studies of oxygenrelated defect formation in neutron irradiated CZsilicon after annealing at T=450650 ℃ under hydrostatic pressure [J]. Materials Science and Engineering. B, 2003, 102(1/3): 339-343.
[11] BORGHESI A, SASSELLA A, GERANZANI P, et al. Infrared characterization of oxygen precipitates in silicon wafers with different concentrations of interstitial oxygen [J]. Materials Science and Engineering. B, 2000, 73(1/3): 145-148.
[12] 孙以材. 半导体测试技术[M]. 北京: 冶金工业出版社, 1984: 241.
[13] 徐进.直拉硅中氧沉淀及其诱生缺陷的透射电镜的研究[D].杭州:浙江大学, 2003: 77.
XU Jin. Transmission electron microscopy investigation of oxygen pre cipitation and induced defects in czochralski silicon \
[D\] Hangzhou:Zhejiang Uriaersity, 2003:77.
[14] FRIGERI C, MA M, IRISAWA T, et al. Analysis of extended defects in nitrogen annealed CZ Silicon by optical and electron beam methods [J]. Materials Science and Engineering. B, 2002, 91:170-173.
[15] XU Yuesheng,LI Yangxian,LIU Caichi,et al.Fast neutron irradiation for Czochralski grown silicon [J].Applied Physics Letters, 1994,65 (22): 2807-2808.
[16] YU Xuegong, YANG Deren, MA Xiangyang, et al.Grown in defects in nitrogen doped Czochralski silicon [J]. Journal of Applied Physics, 2002(92): 188-194.

[1] 刘长殿, 孙红月, 康剑伟, 杜丽丽. 土体的充气阻渗试验[J]. J4, 2014, 48(2): 236-241.
[2] 柯瀚,王文芳,魏长春,陈云敏,詹良通. 填埋体饱和渗透系数影响因素室内研究[J]. J4, 2013, 47(7): 1164-1170.
[3] 余钊圣, 王宇, 邵雪明, 吴腾虎. 中性悬浮大颗粒对湍槽流影响的数值研究[J]. J4, 2013, 47(1): 109-115.
[4] 王林涛,龚国芳,施虎,刘怀印. 基于盾构密封舱压力直接反馈地表变形控制[J]. J4, 2012, 46(7): 1182-1188.
[5] 刘永莉,孙红月,于洋,詹伟,尚岳全. 基于BOTDR监测技术抗滑桩上滑坡推力确定[J]. J4, 2012, 46(5): 798-803.
[6] 林巍, 楼文娟, 申屠团兵, 黄铭枫. 高层建筑脉动风压的非高斯峰值因子方法[J]. J4, 2012, 46(4): 691-697.
[7] 刘永莉, 孙红月, 于洋, 詹伟, 尚岳全. 抗滑桩内力的BOTDR监测分析[J]. J4, 2012, 46(2): 243-249.
[8] 徐日庆,张俊,朱剑锋, 王兴陈. 考虑扰动影响的修正Duncan-Chang模型[J]. J4, 2012, 46(1): 1-7.
[9] 周建, 郑鸿镔, 温晓贵, 管林波, 邓以亮. 考虑中主应力系数影响的主应力轴旋转下
原状软黏土变形研究
[J]. J4, 2011, 45(12): 2134-2141.
[10] 薛文, 金伟良, 横田弘. 养护条件与暴露环境对氯离子传输的耦合作用[J]. J4, 2011, 45(8): 1416-1422.
[11] 陈国红, 谢康和, 程永峰, 徐妍. 考虑涂抹区渗透系数变化的砂井地基固结解[J]. J4, 2011, 45(4): 665-670.
[12] 王艳, 李海峰, 徐熙平. 双灯投影机方棒照明系统的设计[J]. J4, 2011, 45(2): 382-386.
[13] 施虎,龚国芳,杨华勇,汪慧. 盾构掘进机推进力计算模型[J]. J4, 2011, 45(1): 126-131.
[14] 苏锋, 蒋晔, 蔡永昌. 钢管混凝土梁柱节点受力性能有限元分析[J]. J4, 2010, 44(10): 1876-1882.
[15] 朱道建. 柱状节理岩体开挖卸荷效应及破裂区分布规律[J]. J4, 2010, 44(10): 1967-1973.