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J4  2011, Vol. 45 Issue (5): 928-933    DOI: 10.3785/j.issn.1008-973X.2011.05.026
    
Effect of rapid thermal process on oxygen precipitates behavior in
silicon irradiated by high energy particles
CHEN Gui-feng, MA Xiao-wei, WU Jian-hai, MA Qiao-yun,
XUE Jing-jing, HAO Qiu-yan
Key Lab. for new type of functional materials in Hebei Province, School of Material Science and Engineering,
Hebei University of Technology, Tianjin 300130, China
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Abstract  

The oxygen precipitation behavior has been investigated in nitrogen-doped Czochralski silicon (NCZ-Si) irradiated by fastneutron and Czochralski silicon (CZ-Si) irradiated by electron after Rapid Thermal Process (RTP). The samples irradiated by fast-neutron or electron with different dose were treated by post-annealing after RTP pre-annealing at different temperature, cooling rate and ambient. It is found that the RTP process conduces to the denuded zone (DZ) form during the post-annealing treatment in fast-neutron irradiated NCZ-Si wafer. Furthermore, the DZ is getting wider with increasing RTP temperature. On the contrary, the DZ narrowed at high cooling rate. For another thing, the RTP process under N2 ambient in electron irradiated CZ-Si wafer is easy to form the oxygen precipitates and lead to higher density bulk microdefects (BMDS).



Published: 24 November 2011
CLC:  TU 411  
  TU 472.5  
Cite this article:

CHEN Gui-feng, MA Xiao-wei, WU Jian-hai, MA Qiao-yun, XUE Jing-jing, HAO Qiu-yan. Effect of rapid thermal process on oxygen precipitates behavior in
silicon irradiated by high energy particles. J4, 2011, 45(5): 928-933.

URL:

https://www.zjujournals.com/eng/10.3785/j.issn.1008-973X.2011.05.026     OR     https://www.zjujournals.com/eng/Y2011/V45/I5/928


快速热处理对高能粒子辐照硅中氧沉淀的影响

研究快速热处理对快中子辐照掺氮直拉硅(NCZ-Si )和电子辐照直拉硅(CZ-Si)中氧沉淀和清洁区(DZ )的影响.样品经过不同温度、降温速率和退火气氛快速热处理(RTP)预处理后,再进行高温一步长时间退火,以形成氧沉淀.研究结果表明:对于快中子辐照NCZ-Si,RTP有助于后期退火中DZ的生成,且RTP温度越高,形成的DZ越宽;而高的降温速率会使得DZ宽度变窄;对于电子辐照CZ-Si,在N2气氛下高温RTP更能促进氧沉淀形成,体缺陷(bulk micro defects,BMDS)密度较大.

[1] 李养贤,刘何燕,牛萍娟,等. 中子辐照直拉硅中的本征吸除效应[J]. 物理学报, 2002, 51(10): 24072410.
LI Yangxian, LIU Heyan, NIU Pingjuan, et al. The intrinsic gettering in neutron irradiation Czochralskisilicon [J]. Acta Physica Sinica, 2002, 51(10):2410.
[2] SUEZAWA M, SUMINO K, HARADA H, et al. Nitrogenoxygen complexes as shallow donors in silicon crystals [J]. Jpan. Journal of Applied Physics, 1986, 25(52/54): L859-L864.
[3] JIANG Hanqin, MA Xiangyang, YANG Deren, et al. Effect of vacancy on nucleation for oxygen precipitation in conventional and nitrogendoped Czochralski silicon [J]. Journal of Semiconductors, 2008, 29(10): 1984-1987.
[4] LI Yangxian, JU Yulin, LIU Caichi, et al. Inhibition of neutron irradiation on oxidation stacking faults on the surface of Si wafers [J]. J.Cryst.Growth, 1996, 160(3/4): 250-252.
[5] LI Yangxian, GUO H Y, LIU Heyan, et al. The effects of neutron irradiation on the oxygen precipitation in Czochralskisilicon [J]. J.Cryst.Growth, 2003, 253(1/4): 6-9.
[6] Chen Guifeng, LI Yangxian, LI Xinghua, et al. Influence of rapid thermal process on intrinsic gettering in fast neutron irradiated Czochralski silicon [J]. Transactions of Nonferrous Metals Society of China, 2006, 16(1): 109-112.
[7] CHEN Guifeng, MA Xiaowei, BAI Yunna, et al. Effect of oxygen precipitates in annealed electron irradiated Czochralski silicon [C]∥ ISTC/CSTIC 2009 International Semiconductor Technology Conference. Shanghai: The Electrochemical Society, 2009,52-54.
[8] 马巧云. 快中子辐照直拉硅中氧沉淀及诱生缺陷研究[D]. 天津:河北工业大学, 2005: 12-15.
MA Qiaoyun. Investigation of oxygen precipitation and induceddefects in fast neutron irradiated Czochralski silicon [D]. Tianjin: Hebei University of Technology, 2005: 12-15.
[9] QI M W, TAN S S, ZHU B, et al. The evidence for interaction of the NN pair with oxygen in Czochralski silicon [J]. Journal of Applied Physics, 1991, 69: 3775-3777.

[10] SURMA B, LONDOS C A, EMTSEV V V, et al. Infrared studies of oxygenrelated defect formation in neutron irradiated CZsilicon after annealing at T=450650 ℃ under hydrostatic pressure [J]. Materials Science and Engineering. B, 2003, 102(1/3): 339-343.
[11] BORGHESI A, SASSELLA A, GERANZANI P, et al. Infrared characterization of oxygen precipitates in silicon wafers with different concentrations of interstitial oxygen [J]. Materials Science and Engineering. B, 2000, 73(1/3): 145-148.
[12] 孙以材. 半导体测试技术[M]. 北京: 冶金工业出版社, 1984: 241.
[13] 徐进.直拉硅中氧沉淀及其诱生缺陷的透射电镜的研究[D].杭州:浙江大学, 2003: 77.
XU Jin. Transmission electron microscopy investigation of oxygen pre cipitation and induced defects in czochralski silicon \
[D\] Hangzhou:Zhejiang Uriaersity, 2003:77.
[14] FRIGERI C, MA M, IRISAWA T, et al. Analysis of extended defects in nitrogen annealed CZ Silicon by optical and electron beam methods [J]. Materials Science and Engineering. B, 2002, 91:170-173.
[15] XU Yuesheng,LI Yangxian,LIU Caichi,et al.Fast neutron irradiation for Czochralski grown silicon [J].Applied Physics Letters, 1994,65 (22): 2807-2808.
[16] YU Xuegong, YANG Deren, MA Xiangyang, et al.Grown in defects in nitrogen doped Czochralski silicon [J]. Journal of Applied Physics, 2002(92): 188-194.

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