Please wait a minute...
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering)  2004, Vol. 5 Issue (6): 705-708    DOI: 10.1631/jzus.2004.0705
Material & Chemical Science     
Rapid synthesis of ZSM-5 zeolite catalyst for amination of ethanolamine
HUA Yue-ming, HU Wang-ming
Department of Chemical Engineering, Zhejiang University, Hangzhou 310027, China
Download:     PDF (0 KB)     
Export: BibTeX | EndNote (RIS)      

Abstract  ZSM-5 zeolite was rapidly synthesized in system containing ethylenediamine from the initial gel: (5-8) Na2O: 44 EDA:Al2O3:100 SiO2:4000 H2O. The crystals were lath-shaped. The effect of pretreatment and alkalinity on crystallinity was investigated. The pretreatment of silicate source can cut down the crystallization time. Tuning the system alkalinity and controlling crystallization time can ensure forming of pure crystal.

Key wordsZSM-5 zeolite      Synthesis      Pretreatment      Alkalinity     
Received: 07 July 2003     
CLC:  TP2032.4  
Cite this article:

HUA Yue-ming, HU Wang-ming. Rapid synthesis of ZSM-5 zeolite catalyst for amination of ethanolamine. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2004, 5(6): 705-708.

URL:

http://www.zjujournals.com/xueshu/zjus-a/10.1631/jzus.2004.0705     OR     http://www.zjujournals.com/xueshu/zjus-a/Y2004/V5/I6/705

[1] Xiao-zhong Wang, Xia Wang, Ying-qi Chen, Li-yan Dai, Xing-cong Li. Asymmetric synthesis of N-protected 3-methylpiperidin-2-one and its diastereoisomer[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2016, 17(2): 163-170.
[2] Hu Zhang, Cun-lei Wang, Yong Zhang, Jun-yi Liang, Cheng-liang Yin. Drivability improvements for a single-motor parallel hybrid electric vehicle using robust controls[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2014, 15(4): 291-301.
[3] Med Amine Laribi, Lotfi Romdhane, Sa?d Zeghloul. Analysis and optimal synthesis of single loop spatial mechanisms[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2011, 12(9): 665-679.
[4] Xiao-li ZHAN, Bi CHEN, Qing-hua ZHANG, Ling-min YI, Bo JIANG, Feng-qiu CHEN. Synthesis of poly[methyl(3,3,3-trifluoropropyl)siloxane]-b-poly(ethylene oxide) block copolymers[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2008, 9(9): 1304-1308.
[5] Zeng-he LI, Hai-dan BAI. Hydrothermal synthesis and characterization of two novel inorganic-organic hybrid materials[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2008, 9(1): 143-148.
[6] Yu-Feng Liao , Wen-Jiang Li. Synthesis of CdSe quantum dots via paraffin liquid and oleic acid[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2008, 9(1): 133-136.
[7] CHAI Deng-feng, PENG Qun-sheng. Stepwise approach for view synthesis[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2007, 8(8): 1218-1226.
[8] LIU Peng, XIA Bing-jie, TENG Zhao-wei. Physical design method of MPSoC[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2007, 8(4): 631-637.
[9] JIANG Xiao-yuan, DU Feng, ZHANG Xu, JIA Yan-rong, ZHENG Xiao-ming. Catalytic properties of CuO/Sn0.9Ti0.1O2 and CuO/Sn0.7Ti0.3O2 in NO+CO reaction[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2007, 8(11): 1839-1845.
[10] WANG Ji-min, PAN Xue-zeng, WANG Jie-bing, SUN Kang. Fast combination of scheduling chains under resource and time constraints[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2007, 8(1 ): 17-.
[11] Wei Bao-gang, Li Jian-ping, Pang Xiang-bin. Using texture synthesis in fractal pattern design[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2006, 7(3 ): 2-.
[12] ZHANG Yan-hu, YAN Wen-jun, LU Jian-ning, ZHAO Guang-zhou. Multi-objective robust controller synthesis for discrete-time systems with convex polytopic uncertain domain[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2005, 6(Supplement 1): 87-93.
[13] LI Jian-hua, LIU Yu-sheng, GAO Shu-ming. Mask synthesis and verification based on geometric model for surface micro-machined MEMS[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2005, 6( 8): 17-.
[14] XIE Fei, YANG Hui, XU Cun-jin, ZHANG Xi-he. In-situ synthesis and luminescence properties of titanium oxide gels containing 1,10-phenanthroline europium(III) complex*[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2005, 6( 7): 1-.
[15] TONG Shao-ping, WEI Hong, MA Chun-an, LIU Wei-ping. Rapid dechlorination of chlorinated organic compounds by nickel/iron bimetallic system in water*[J]. Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2005, 6( 7): 3-.