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POLYMERIZATION OF METHYL METHACRYLATE WITH ETHYLENE BRIDGED HETERODINUCLEAR METALLOCENE OF SAMARIUM AND TITANIUM—STUDY ON SYNERGISM AND KINETICS
SUN Jun-quan, PAN Zhi-da, HU Wei-qiu, YANG Shi-lin
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 366-371.
https://doi.org/10.1631/jzus.2001.0366
Comparison of MMA polymerization results with samarocene chloride, titanocene chloride and the title heterodinuclear (Sm-Ti) catalyst, respectively, showed synergism in the Sm-Ligand-Ti system, which obviously influenced the polymerization behaviors, for example, of yielding higher activity and higher molecular weight polymer. Kinetic studies on polymerization of MMA with ethylene bridged samarocene and titanocene chloride/M(i-Bu)3 showed that the polymerization rate was first-order on the catalyst concentration, and 1.9-order on the monomer. The overall activation energy measured was 52.8 kJ/mol.
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CONFORMATION AND MICROSTRUCTURE OF CARBON NANOFIBERS DEPOSITED ON FOAM Ni
LU Xiao-nan, DENG Fu-min, CHEN Xiao-hua, ZHANG Xiao-bin, WANG Miao, LI Wen-zhu
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 372-375.
https://doi.org/10.1631/jzus.2001.0372
Bundles of pure carbon nanofibers were prepared by catalytic decomposition of acetylene on foam Ni. The morphological and structural characteristics of the carbon nanostructures, in the as-prepared state, were analyzed by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and high resolution transmission electron microscopy (HTEM). A special conformation of carbon nanofibers composed of segmented structures was found among the products by both SEM and TEM observations. Further HTEM examination indicated that the segments were stacked with well ordered graphite platelets arranged perpendicular to the axis of the filaments.
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ANOMALOUS HOPPING AND TUNNELING EFFECTS IN A NEW ALUMINUM FILM PERCOLATION SYSTEM
XIA A-gen, YE Jian-ting, YE Quan-lin, TAO Xiang-ming, JIN Jin-sheng, YE Gao-xiang
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 379-383.
https://doi.org/10.1631/jzus.2001.0379
A new aluminum thin film percolation system, deposited on glass and silicon wafer surfaces by a vapor deposition method, was investigated. By using the expansive and mobile behaviors of the silicone oil, the Al films are quenched gradually by the silicone oil during the deposition process, The R-I behavior of the film system was studied, and the anomalous conductivity indicated that, at very low current, the hopping and tunneling effects in the films are much stronger than those of the normal film systems.
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USE OF SUPERPOSITION PRINCIPLE TO DERIVE A GENERAL MATHEMATICAL MODEL TO SIMULATE ONE-TO-ONE, ONE-TO-MULTI AND MULTI-TO-MULTI SAW FILTER DESIGNS
Issa Haitham M.A., ZHU Da-zhong, QIU Pei-liang
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 395-400.
https://doi.org/10.1631/jzus.2001.0395
This paper explains and summarizes a new attempt to derive a general mathematical model [GMM] to simulate surface acoustic wave (SAW) filters, using the superposition principle and delta function model. GMM can be used to simulate One-to-One, One-to-Multi and Multi-to-Multi SAW filter devices. The simulation program was written using MATLAB (the language of technical computing). Four-design structures (One-to-One, One-to-Two, One-to-Three and Ten-to-Ten) are selected to test the correctness of GMM. The frequency response of the simulation and test results are similar in center frequency and 3-dB bandwidth, but the insertion loss is different, because of some second order effects (Issa Haitham, 1999).
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VIRTUAL INSTRUMENT SYSTEM SOFTWARE ARCHITECTURE DESCRIPTION LANGUAGE
ZHOU Hong, WANG Le-yu
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 411-415.
https://doi.org/10.1631/jzus.2001.0411
In software engineering, an architecture description language (ADL) is intended to aid designers in defining software architectures in terms of abstractions that they find useful, and in making a smooth transition to code. Based on ADL, the concept and models of the Virtual instrunent system Software architecture Description Language (VSDL) is provided in this paper. The VSDL put forward provides a new method for virtual instrunent system\'s application design and development by describing the virtual instrument system software architecture effectively. In this paper, the model description, component description and line description are analyzed in detail, and the structure language based on the model is also provided. VSDL provides a smooth interface to graphic software platform, and has been applied to many virtual instrument systems\' integration and already yielded good results both in technology and economy.
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COMPARISON OF DIFFERENT ENZYMES AND PROBES AND THEIR COMBINATIONS IN DNA FINGERPRINTING
FU Yan, NIU Dong, RUAN Hui, CHEN Haiyan, Ponsuksili S., Horst P.
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 431-435.
https://doi.org/10.1631/jzus.2001.0431
In the present study, eight combinations of restriction enzymes and oligonucleotide probes were tested for detecting VNTR polymorphism. More than a hundred loci were detected by all enzyme-probe combi nations. The influences of breed, enzyme and probe as well as their interactions were analysed, and the mean value of DNA fingerprint data was calculated for the enzymes and probes. The results will provide some valuable information for studying the genetic relationship of individuals or populations using DNA fingerprinting.
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LONG-TERM INHIBITION OF Na+/H+ EXCHANGE ATTENUATES CARDIAC REMODELING AFTER MYOCARDIAL INFARCTION IN RATS
XIA Qin-gui, Oliver Chung, Heidi Spitznagel, Thomas Unger
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 439-444.
https://doi.org/10.1631/jzus.2001.0439
Objective: In addition to pH regulation, Na+/H+ exchanger (NIE) has been shown to facilitate cell growth and proliferation. However, the effects of long-term inhibition of Na+/H+ exchange on cardiac structural and functional remodeling post myocardial infarction (MI) are still controversial. The present study was therefore carried ont to further investigate the effects of long-term treatment with cariporide, a specific inhibitor of NHE-1, on cardiac remodeling after MI in rots; Methods: Male Wistar rots that underwent coronary ligation were randomly selected for cariporide treatment starting 6 h after induction of MI or no treatment. Treatment was continued up to 6 weeks post MI, after which, the arterial, venous and left ventricular catheters were chronically implanted. Twenty-four h later, after hemodynamic signals were recorded in conscious rats, they were sacrificed and hearts were taken out for morphological examinations; Results: Cariporide treatment decreased the heart weight and heart weight to body weight ratio (both P<0.05), decreased left ventricular end-diastohc pressure (P<0.001), improved myocardial contractility (dP/dtmax) (P<0.05) and tended to increase the survival of treated rots compared to that of untreated infarct rats; Conclusion: The results of the present study indicate that the long-term inhibition of NHE with cariporide can attenuate cardiac structural re-modeling and improve left ventricular dysfunction in infarcted rats, and suggest that Na+/H+ exchange inhibition could be an effective therapeutic strategy for myocardial infarction-induced heart failure.
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CONSTRUCTION AND IDENTIFICATION OF THE RECOMBINANT OF THE AAV VECTOR AND HUMAN INTERFERON-GAMMA
ZHU Hai-hong, CHEN Zhi, ZHANG Ming-tai, DING Lie-ming
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 445-447.
https://doi.org/10.1631/jzus.2001.0445
To construct and identify further a recombinant of Adeno-associated virus and interferon-gamma for gene therapy, the full-length IFN-γcDNA containing signal peptide was amplified by PCR, and then cloned into the pUC18. After screening, the fragment from the positive clone was then subcloned into pwpl9. After the correct recombinant was identified by digestion with SacI and BamHI, it was transfected into lymphocyte cell line H9 mediated by calcium phosphate, and the expression of IFN-γ was detected by RT-PCR and ELISA. The result showed that the IFN-γ were expressed in the H9 cells transfected with pwp/IFN-γ. The so constructed recombinant plasmid pwpl9/IFN-γ containing the full-length IFN-γ gene was expressed in mammalian cells.
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CHANGES OF OXIDATIVE AND LIPOPEROXIDATIVE METABOLISM IN PATIENTS WITH ACUTE VIRAL MYOCARDITIS
CHEN Peng, ZHOU Jun-fu
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 448-452.
https://doi.org/10.1631/jzus.2001.0448
Objective: To study the changes of oxidative metabolism and lipoperoxidative metabolism in patients with acnte viral myocarditis (AVM), and to research pathological chain reactions of a series of free radicals, and oxidative damage and lipoperoxidative damage in AVM patients\' bodies. Methods: A random paired control design was used to investigate 70 cases of AVM patients and 70 cases of healthy adult volunteers (HAV) on the basis of contents of nitric oxide (NO), lipoperoxide (LPO) in plasma, and LPO in red blood cell (RBC) as well as activities of superoxide dismutase (SOD), catalase (CAT) and glutathione peroxidase (GSH-Px) in RBC as revealed by spectrophotometric assays. Results: Compared with the average values (AV) of the above biochemical parameters (BP) in the HAV group, the AV of NO in plasma, and LPO in plasma and in RBC in the AVM group were significantly increased (P=0.0001), while the AV of SOD, CAT and GSH-Px in the AVM group were significantly decreased (P=0.0001). Conclusion: The findings in this study suggested that in the AVM patients bodies the metabolism of NO was disturbed, and the pathological chain reactions of a series of free radicals were so severely aggravated, as to cause the oxidative damage and lipoperoxidative damage in the AVM patients\' bodies.
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MOTILIN LEVELS AND ELECTROGASTROENTEROGRAM STUDIES IN HYPOTHYROIDISM
WANG Hang-yong, CAO Qian, LI You-ming
Journal of Zhejiang University-SCIENCE A (Applied Physics & Engineering), 2001, 2(4): 453-455.
https://doi.org/10.1631/jzus.2001.0453
To study the relationship between gastrointestinal dysfunction and motilin in patients with hypot- hyroidism. The plasma motilin concentration was measured by radiommunoassay(RIA) in 30 patients with hypothyroidism and also in 30 controls. At the same time, the electrogastroenterogram was also taken. Among the hypothyroidism patients, 56.6% had decreased gastric motility, especially in gastric body and greater gastric curvature; 86.6 % had decreased colonic motility, especially in the left half of the colon. There were no significant differences of plasma motilin concentration between patients with hypothyroidism and controls (P>0.05). There were also no differences between pre-treatment and pest-treatment individuals, but significant differences were observed in the electrogastroenterogram. We conclude that the plasma motilin eoncertration in hypothyroidism patients was the same as that in normal patients, and that electrogastmenterogram studies in patients with gastrointestinal dysfunction may be valuable.
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26 articles
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